METHOD FOR RECOVERING MERCURY
FROM FIXING FLUIDS.
DRAFT COPY ONLY.
(Procedure 22).
http://www.netautopsy.org/axsop/axsop022.htm


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United States Government Work, uncopyrighted, public-domain, DRAFT COPY ONLY. This document does not necessarily represent the views or policies of any United States Government agency. This document is provided "as is", without warranty of any kind, express or implied, including but not limited to the warranties of merchantability, fitness for a particular purpose and non-infringement. In no event shall the authors be liable for any claim, damages or other liability, whether in an action of contract, tort or otherwise, arising from, out of, or in connection with the document or the use or other dealings made with the document.

See also: Main objectives: 1.
Mercury removal: 21.



PRINCIPLE OF THE TEST.


Treatment of specimens received in a mercury-containing fixative that were prepared off-site.



SPECIMEN REQUIRED.


All human tissue excised at surgery, outpatient clinics, and postmortems, fresh or in fixative, along with a filled-out Tissue Examination Form (U. S. Standard Form 515, USSF515).



REAGENTS, INSTRUMENTATION.

      13% Thioacetamide. Fluted filter paper.



STEP-BY-STEP DESCRIPTION.


1. Mercury-containing fixatives are not recommended by the Department of Pathology, and are not distributed or prepared by the Department of Pathology. Occasionally, a specimen comes in a mercury-containing fixative that was prepared off-site. In this case, the following protocol is used to recover mercury.

2. To each liter of B5 or Zenker's waste, add 20ml of a 13% solution of thioacetamide. Mix thoroughly and allow to stand in hood.

3. Filter with fluted filter paper in hood.

4. Discard the clear filtrate in the sink with copious amounts of water.

5. The residue containing mercuric salt can be stored in a glass jar indefinitely.



REFERENCE.


1. Prophet EB, Mills B, Arrington JB, Sobin LH.
Laboratory Methods in Histotechnology, pp. 25-28.
1992: Armed Forces Institute of Pathology, Washington, DC. 20306-6000.
ISBN: 1-881041-00-X 1992.